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Untitled Document

 
  AGRONOMY & SOILS SERIES

TIMELY INFORMATION

Agriculture & Natural Resources
DEPARTMENT  OF  AGRONOMY  &  SOILS,  AUBURN  UNIVERSITY,  AL  36849-5633


S-03-98 June, 1998


Manure Testing for Fertilizer


Charles C. Mitchell, Extension Agronomist-Soils and
Hamilton H. Bryant, Lab Director


     Some Alabama livestock producers are faced with mandatory nutrient and waste management planning as a result of impending CAFO (confined animal feeding operations) and AFO (animal feeding operations) regulations. As a result, there will be a greater demand for manure and animal waste testing services. The Soil Testing Laboratory at Auburn University has offered manure testing services since 1991. However, producer demand for these services has been light. On an average annual basis, the lab has run about 80 poultry broiler litter samples, 10 liquid lagoon samples and 10 other manure samples. In addition, about 50 by product and compost samples are tested each year for land application. These numbers are expected to increase dramatically with CAFO regulations.

Who should be responsible for sampling and testing manure?

     Sampling, testing, and guaranteeing the analysis is the responsibility of the person who produces the manure and/or the person who sells or spreads it for someone else. Landowners should never accept a "free" material or buy manure without first asking for a laboratory analysis from the person who produced the manure or is distributing the manure.

Why should manures be sampled?

Poultry broiler litter. Some manures are more variable than others. Dry, poultry broiler litter is, perhaps, the most consistent manure produced in Alabama. It has an average fertilizer value equivalent to a 3-3-2 fertilizer when it comes out of the house. But the number of flocks raised on the litter, type of bedding, and storage and handling facilities can affect the actual analysis of each batch of litter. Producers can do an acceptable job of land application assuming the average analysis of 3-3-2 or 60-60-40 pounds N-P2O5-K2O per ton for fresh litter applied directly from the house (see Extension Cir. ANR-0244). However, if one is buying or selling broiler litter, periodic testing would protect both the buyer and seller and establish a documented basis for the nutrient management plan.

Layer and breeder litter/manures. Manure from these birds are handled differently by each producer and integrator. Routine samples over a period of time by the producer can establish the variability for each production system.

Dairy and swine lagoon effluents. These are the most variable from one farm to another. Average values are of little use in a nutrient management plan. The effluent being applied should be tested regularly from each unit until relatively consistent analyses are established.

Feedlot and stable manures. These are also highly variable from one operation to another. However, once a base value is established for a feeding operation, manure will not have to be tested as frequently.

Composted manures. The composting process greatly alters the concentration and availability of plant nutrients. Dry manures must be moistened in order to compost properly and this reduces the nutrient concentration on an as-sampled basis. All composted manures should be sampled regularly until a reasonable value can be established for each process.

Other organic amendments. Municipal biosolids (sludges), industrial by-products for land application, urban yard wastes, composted yard wastes, septage, and other types of organic materials for land application should be regularly tested for is fertilizer value. Alkaline materials should also be evaluated for their agricultural lime value (wood ash, paper mill lime, lime-activated biosolids, etc.)

How should manures be sampled?

Fresh poultry broiler litter. Take a handful of litter from 15 to 20 spots throughout the house as the litter is being removed. Mix these in a clean, plastic bucket and put about 1 quart in a heavy duty plastic freezer bag to send to the laboratory.

Dry-stacked or stored poultry litter. Using a shovel, dig into the stack 2-3 feet and take about a handful of litter from within the stack. Repeat this at 10-20 spots around the stack. Mix these subsamples in a clean, plastic bucket and put about 1 quart in a heavy duty plastic freezer bag to send to the laboratory.

Layer and breeder litter/manures. Sample the same as for fresh or stored poultry litter.

Dairy and swine lagoon slurry from under-slotted-floor pit. (see Extension Cir. ANR 1102). Extend a ½-inch nonmetallic conduit that is open on both ends into the manure all the way to the pit floor. Place your thumb over the upper end of the conduit to seal it to trap the manure that has entered the lower end. Remove the conduit from the pit and empty the slurry into a plastic bucket. Repeat this from 5 or more locations. Mix well and save about 1 quart in a clean, plastic bottle for the laboratory. Refrigerate or freeze until sample can be delivered to the laboratory.

Dairy and swine lagoon slurry from outside storage lagoon or tank. Mix the manure well using a liquid manure chopper pump or propeller agitator. Continuous agitation for at least 12 hours is necessary for a lagoon or storage pond to be properly mixed. Take subsamples from about 5 locations around the lagoon or from the output from the agitator pump or propeller agitator, or from the manure spreader. Mix the subsamples in a plastic bucket and save at least 1 quart for the laboratory. This should be put into a clean, plastic bottle (such as a soft drink bottle with a plastic screw cap). Refrigerate or freeze the sample until delivery to the laboratory.

Dairy and swine lagoon liquid effluent. From the recycle system, collect about 1 pint from the inflow pipe to the flush tanks. From the lagoon, place a small bottle (about ½ pint) on one end of a 10- to 15-foot pole. Extend the bottle 10 to 15 feet away from the edge of the lagoon. Brush away any floating debris, and submerge the bottle within 1 foot of the surface. Retrieve the bottle, and empty it into a plastic bucket. Repeat this process about 5 times around the lagoon; mix the samples and pour about 1 quart into a clean, plastic bottle (such as a soft drink bottle with a plastic screw cap) and refrigerate or freeze until delivery to the laboratory.

Feedlot and stable manures (semi-solid manures). After manures are scraped into a spreader, collect about 2 pounds of manure from different locations in the spreader. Mix these in a clean, plastic bucket and put about 1 quart in a heavy duty plastic freezer bag or plastic bottle to send to the laboratory.

Composted manures. Sample the same as dry-stacked or stored poultry litter.

Other organic amendments. Try to get a representative sample by collecting 10-20 subsamples from throughout the stack, pile, bin, lagoon, etc. Mix the subsamples in a clean, plastic bucket and submit at least 1 quart to the laboratory for analysis. Samples may be dried if moisture is of no concern.

What should I expect on a manure analysis?

     The Auburn University laboratory will give you the following information on the sample as it was submitted (see attached sample reports)

Moisture (%)
Ash (%). This gives the amount of inert material such as soil that may contaminate the sample; the higher the ash, the lower the fertilizer value.
Dry litter analysis: total N, P, K, Mg, Ca, Cu, Zn, B
Liquid lagoon analysis: total N, ammonium-N, P, K, Ca, Mg, Cu, Fe, Mn, Zn, B, Mo, Al, Ba, Co, Cr, Pb, Na
Fertilizer grade expressed as percentage total N-P2O5-K2O
Total N-P2O5 -K2O expressed as pounds per ton or pounds per 1,000 gallons for liquid samples.

     Certain other analyses could be run on the sample but must be requested such as total sulfur (S), neutralizing value (lime value), nitrate-nitrogen and soluble salts.

What does it cost?

     The routine manure analysis is $25 per sample. Additional analyses are approximately $5 per analysis.



Example of lagoon waste analysis

Example of poultry litter analysis for fertilizer value

 

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